Materials Physics and Engineering

How can we make today’s materials safer and more efficient? Can we combine key experiments with computational tools to design and engineer new materials? Such questions, which are at the core of materials research, are addressed with x-rays by users and staff of the Materials Physics and Engineering (MPE) group.

The MPE group operates 1-ID, 6-BM (in partnership with COMPRES), and 6-ID-D (50% of the time; high-throughput high energy diffraction microscopy program) and develops a variety of in situ x-ray imaging and scattering techniques so that materials can be characterized at multiple length scales simultaneously and non-destructively.

 
08.13.2014
Raloxifene, a treatment for decreasing fracture risk in osteoporosis, works only partially by suppressing bone loss. Studies at the U.S. Department of Energy′s Advanced Photon Source revealed an add...
1-ID-B,C,E
12.10.2014
Understanding how cracks spread through a material is important for predicting how long a structure might last before breaking, as well as for designing new materials more resistant to failure. Resear...
1-ID-B,C,E
12.15.2015
The smooth, metallic surface of a titanium golf club head hides a messy reality. Though it looks homogenous to the naked eye, the head is actually made of individual grains of metal, of many different...
1-ID-B,C,E
02.04.2016
Cast iron is an alloy of iron, carbon, silicon, and other elements with numerous industrial and consumer applications. The carbon content of cast iron — generally higher than that of steel — appea...
1-ID-B,C,E
12.03.2013
Humans have devised many amazing and versatile materials (such as plastic and steel) that do not exist in nature. On the other hand, nature has created structures and substances that materials scienti...
1-ID-B,C,E
03.03.2009
Power plants based on turbine engines burning natural gas are a key component of future energy grids in the U.S. and other nations. With these engines, power plants will supply clean, increasingly fue...
1-ID-B,C,E
10.22.2010
Research at the U.S. Department of Energy’s Advanced Photon Source (APS), Center for Nanoscale Materials (CNM), and Electron Microscopy Center (EMC) at Argonne National Laboratory has provided an un...
1-ID-B,C,E
11.28.2017
APS Group Leader Jonathan Almer, left, takes measurements during an experiment on Monday to study a nearly 2,000 intact mummy that was found in Egypt. The powerful x-ray beams at the APS could shed li...
1-ID-B,C,E
03.06.2018
Titanium is a workhorse metal of the modern age. Alloyed with small amounts of aluminum and vanadium, it is used in aircraft, premium sports equipment, race cars, space craft, high-end bicycles, and m...
1-ID-B,C,E
03.15.2018
From detecting x-rays from outer space to elemental mapping at the nanoscale, transition-edge sensors (TES) are essential tools for scientific discovery. These devices measure the electrical resistan...
1-ID-B,C,E
09.20.2018
In work that could help prevent the failure of everything from bridges to dental implants, a team of researchers utilized the U.S. Department of Energy’s Advanced Photon Source to obtain the first t...
1-ID-B,C,E
10.24.2018
Although crucial to modern life, metal alloys can fail, possibly leading to bridge collapse or other disasters. One cause of failure about which little has been understood is hydrogen embrittlement, w...
1-ID-B,C,E
06.02.2020
Understanding the primary mechanisms responsible for steel embrittlement caused by H2 exposure should help materials scientists develop strategies to ameliorate this problem, which has important ramif...
1-ID-B,C,E
07.20.2020
Research at the U.S. Department of Energy’s Advanced Photon Source Stress revealed new information about wave propagation through granular material, which is important for detecting the magnitude of...
1-ID-B,C,E
08.06.2020
Researchers using the U.S. Department of Energy’s Advanced Photon Source took a detailed look at high-temperature tantalum behavior to assess its role in potential future superconducting, optoelectr...
1-ID-B,C,E, 11-ID-C
06.08.2021
Testing the Mettle of Lithium Metal Batteries: Lithium-based batteries need improvement. Researchers used the U.S. Department of Energy’s Advanced Photon Source to gather information which could le...
1-ID-B,C,E
10.18.2021
Multi-Scale Experiments Inform Modeling of Titanium Alloy Durability: Titanium alloys have been widely used in the biomedical and aerospace industries for decades, but the mechanisms associated with ...
1-ID-B,C,E
02.22.2022
BraggNN: Deep Learning for X-ray Diffraction Microscopy: Artificial intelligence (AI) systems using deep-learning neural networks are revolutionizing many scientific disciplines. Researchers at the...
1-ID-B,C,E
10.03.2022
How to 3D-Print One of the Strongest Stainless Steels: Many critical technologies contain a remarkably strong and corrosion-resistant alloy called 17-4 precipitation hardening stainless steel. Based ...
1-ID-B,C,E, 9-ID-B,C
11.14.2022
New System to Visualize 3-D Metal Printing Process May Tap Its Unrealized Potential: The additive manufacturing technique electron beam-powder bed fusion (EB-PBF) has grown rapidly in recent years. R...
1-ID-B,C,E, 32-ID-B,C
01.30.2023
The More Things Change, the More They Become the Same in Uranium-Niobium: Experimenters used synchrotron x-ray studies at the U.S. Department of Energy’s Advanced Photon Source to investigate the ...
1-ID-B,C,E
 

 

1-ID

1-ID beamline is an insertion device beamline capable of delivering monochromatized high-energy x-rays above 42 keV, providing a unique combination of penetration power and high spatio-temporal resolution.

These characteristics are exploited with three primary techniques

(i) high-energy diffraction microscopy (HEDM), 

(ii) combined high-energy small- and wide-angle x-ray scattering (HE-SAXS/WAXS), and 

(iii) high-energy tomography.

HEDM reveals information on individual grains (size, shape, orientation, strain) within polycrystalline aggregates, while HE-SAXS/WAXS reveals similar grain-averaged information over a wide range of size scales (0.1-100 nm). Incident x-ray beams can be focused down to the micron-level, and 3-dimensional information can be achieved either in direct space, using a conical-slit system (~100 micron resolution), or through reconstruction algorithms. These techniques rely on area detectors for efficient data collection with temporal resolutions down to 10msec, and are often used with thermo-mechanical environments, to enable studies of ‘real materials in real conditions’.

High-energy tomography is often combined with the scattering techniques to obtain a multi-modal 3D picture of a material.

1-ID experiment examples

 

6-BM

6-BM experiment example

6-BM is a bending magnet beamline capable of delivering polychromatic high-energy x-rays that are used for

(i) energy dispersive diffraction (EDD) and

(ii) tomographic imaging.

These techniques are combined to characterize the internal structure and state of complex material systems like batteries, bones, and large machine components.

6-ID-D

6-ID-D is an insertion device beamline capable of delivering monochromatized high-energy x-rays. It is equipped with the high-throughput high-energy diffraction microscopy (HT-HEDM) equipment and computing infrastructure to provide ex situ HEDM characterization capabilities to the user community.

The HT-HEDM equipment consists of

(i) Near- and far-field HEDM

(ii) tomographic imaging.